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Table. 1.

Table. 1.

1H (700 MHz) and 13C (150 MHz) NMR data of 1 in CD3OD:CDCl3 = 1:1.

Position 1 Position 1
δC, type δH, mult. (J in Hz) δC, type δH, mult. (J in Hz)
1 172.4, Cb 1' 172.4, Cb
2 2'
3 78.7, CH 4.86, m 3' 78.7, CH 4.86, m
4 33.4, CH2 3.19, m
3.06, m
4' 33.4, CH2 3.19, m
3.06, m
4a 133.8, C 4a' 133.8, C
5 117.3, CH 7.05, s 5' 117.3, CH 7.05, s
5a 141.0, C 5a' 141.0, C
6 99.0, CH 6.76, s 6' 99.0, CH 6.76, s
7 162.6, C 7' 162.6, C
8 109.0, C 8' 109.0, C
9 155.8, C 9' 155.8, C
9a 109.0, C 9a' 109.0, C
10 163.8, C 10' 163.8, C
10a 100.2, C 10a' 100.2, C
11 56.4, CH3 3.82, s 11' 56.4, CH3 3.82, s
12 42.7, CH2 2.10, m
1.92, m
12' 42.7, CH2 2.10, m
1.92, m
13 68.6, CH 4.10, ma 13' 67.8, CH 4.10, ma
14 44.8, CH2 1.61, ma 14' 43.7, CH2 1.66, ma
1.59, ma
15 72.1, CH 3.80, m 15' 70.8, CH 4.05, m
16 38.6, CH2 1.44, ma 16' 44.2, CH2 1.67, ma
1.59, ma
17 26.0, CH2 1.42, ma
1.30, ma
17' 71.3, CH 4.03, m
18 30.3, CH2 1.24, ma 18' 44.3, CH2 1.59, ma
1.52, m
19 30.3, CH2 1.24, ma 19' 71.6, CH 3.77, m
20 32.5, CH2 1.25, m 20' 40.7, CH2 1.42, ma
21 23.3, CH2 1.27, m 21' 19.2, CH2 1.41, ma
1.34, ma
22 14.4, CH3 0.86, dd (8.5, 5.3) 22' 14.4, CH3 0.90, dd (8.5, 5.3)

aResonances overlapped

bPeaks only detected in HMBC

J. Microbiol. Biotechnol. 2023;33:1437~1447 https://doi.org/10.4014/jmb.2301.01017
© J. Microbiol. Biotechnol.